Life Sciences
New life sciences findings from Dr. Babasaheb Ambedkar Marathwada University, Department of Chemical Technology described
Published in Drug Law Weekly, December 2nd, 2008
Investigators publish new data in the report 'Development and validation of chiral LC method for the enantiomeric separation of duloxetine on amylose based stationary phase.' "A simple, rapid, and robust liquid chromatography method was developed and validated for the enantiomeric separation of duloxetine in bulk drug substance. The enantiomers of duloxetine were resolved on a Chiralpak AD-H (amylose based stationary phase) column using a mobile phase consisting of n-hexane-ethanol-diethyl amine (80:20:0.2, v/v/v) at a flow rate of 1.0 mL/min," scientists in India report.
"The resolution between the enantiomers was found to be not less than 2.8 in optimized method. The...
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Source: Drug Law Weekly (2008-12-02)
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